摘 要:
从理论上分析了采用真空蒸馏的方法将粗硒提纯除杂的可行性和规律性,通过小型实验考察了蒸馏温度和时间两个因素对提纯效果的影响.确定最佳工艺条件为:蒸馏温度483K,蒸馏时间20min,可获得硒的品位为99%以上。[著者文摘]

文章出处:
《昆明理工大学学报:理工版》-2006年31卷3期 -26-28页
Journal of Kunming University of Science and Technology(Natural Science Edition)
栏目信息:
分 类 号:
文献标识码:
A
文章编号:
1007-855X(2006)03-0026-03
[参考文献]
Study on Obtaining Pure Selenium by Vacuum Distillation
WAN Wen, YANG Bin, LIU Da-chun , LIU Yong-chen, DU Guo-shan, TANG Wan-qi, LIU Yuan-yuan(Research Institute of Vacuum Metallurgy and Materials, Kunming University of Science and Technology, Kunming 650093, China)
Abstract:
A new technique has been researched on the feasibility and regularity for removing impurities from rude selenium by vacuum distillation in theory analysis. The influence of distillation temperature and time on the effect of purifying selenium is investigated by diminutive experiments. The optimal technical condition is achieved as following: distillation temperature is 483K and distillation time is 20 min. Results show that the content of selenium is more than 99%.[著者文摘]
Key words:
selenium; vacuum distillation; saturation vapor pressure
收稿日期: 2005-05-13

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