学术
国际标准刊号：ISSN 1000-0720
国内统一刊号：CN 11-2017
摘 要:
采用HD-8微色谱柱对高稀土铁矿石样品（白云鄂博矿）中的钍进行分离富集,探讨了影响其分离富集的条件。实验表明,在4 mol/L HCl介质中钍可被树脂完全吸附,用3 mL 40 g/L草酸铵溶液可以从吸附柱上完全解吸钍,并结合偶氮胂Ⅲ分光光度法进行测定。所建立的方法适合于含铁、稀土量高的矿石样品中微量钍的分离与测定。[著者文摘]
文章出处:
《分析试验室》-2008年27卷3期 -52-55页
Chinese Journal of Analysis Laboratory
栏目信息:
分 类 号:
文献标识码:
A
文章编号:
1000-0720（2008）03-052-04
[参考文献]
Separation of thorium in lanthanon-iron ore samples by microcolumn of HD-8 resin and determination by spectrophotometry
YANG Zhi, LI Bo-ping, LUO Ming-biao , SONG Jin-ru, LIU Wei （Applied Chemistry Department, East China Institute of Technology, Fuzhou 344000）
Abstract:
The optimum conditions of separation and preconcentration for thorimn are studied in this paper. Thorimn is adsorbed by HD-8 resin in 4 mol/L HC1 solution, and eluted completely by using 3 mL of 4% ammonimn oxalate, then determined by spectrophotometry. The method is simple, accurate and applicable to the separation and determination of trace thorimn in lanthanoniron ore samples.[著者文摘]
Key words:
Microcolunm; Separation; Preconcentration; Lanthanon-iron ore; Thorimn
收稿日期: 2006-12-25
修订日期: 2007-01-31
基金资助:
核资源与环境教育部重点实验室开放基金、白云额博矿钍的赋存状态与溶出规律研究（60612）项目资助
更多评论>>文章评论
更多>>免费文章
cqvip.com